37148-47-3

  • Product Name:4-Amino-3,5-dichloro-alpha-bromoacetophenone
  • Molecular Formula:C8H6BrCl2NO
  • Purity:99%
  • Molecular Weight:
Inquiry

Product Details;

CasNo: 37148-47-3

Molecular Formula: C8H6BrCl2NO

Appearance: White fine powder

Delivery Time: Delivery within one week after order confirmation

Throughput: 1|Metric Ton|Day

Purity: 99%

Reputable Quality Manufacturer Supply Best Quality 37148-47-3 On Stock with Safe Transportation

  • Molecular Formula:C8H6BrCl2NO
  • Molecular Weight:282.952
  • Appearance/Colour:Yellow solid 
  • Vapor Pressure:1.71E-06mmHg at 25°C 
  • Melting Point:142-145 °C 
  • Refractive Index:1.643 
  • Boiling Point:396.4 °C at 760 mmHg 
  • PKA:-2.21±0.10(Predicted) 
  • Flash Point:193.6 °C 
  • PSA:43.09000 
  • Density:1.764 g/cm3 
  • LogP:3.73440 

4-Amino-3,5-dichloro-alpha-bromoacetophenone(Cas 37148-47-3) Usage

Preparation

Dissolve 4-amino-3, 5-dichloroacetophenone in chloroform and heat to 65°C. Add bromine dropwise with stirring, stir for a few minutes after adding, then add ethanol and stir. Freeze, filter out the crystals, wash with chloroform, and dry at low temperature to obtain finished products.

 

 

InChI:InChI=1/C8H6BrCl2NO/c9-3-7(13)4-1-5(10)8(12)6(11)2-4/h1-2H,3,12H2

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37148-47-3 Process route

C<sub>8</sub>H<sub>5</sub>Br<sub>2</sub>Cl<sub>2</sub>NO

C8H5Br2Cl2NO

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

Conditions
Conditions Yield
With triethylamine; phosphonic acid diethyl ester; In tetrahydrofuran; at 0 - 20 ℃; for 3h;
4.25 g
1-(4-amino-3,5-dichlorophenyl)-1-ethanone
37148-48-4

1-(4-amino-3,5-dichlorophenyl)-1-ethanone

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

C<sub>8</sub>H<sub>5</sub>Br<sub>2</sub>Cl<sub>2</sub>NO

C8H5Br2Cl2NO

Conditions
Conditions Yield
With bromine; In chloroform; for 0.25h; Reflux;
42%
28%

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